Abstract
A redox titrator for the preparation of small volumes of highly concentrated biological samples for X-ray synchrotron studies provides for the redox equilibration at temperatures of 40 to -30°C. Anaerobic transfer directly to the X-ray sample chamber and mixing of an additional reagent just prior to freeze-trapping of the redox-equilibrated sample are provided.
| Original language | English (US) |
|---|---|
| Pages (from-to) | 239-247 |
| Number of pages | 9 |
| Journal | Analytical Biochemistry |
| Volume | 124 |
| Issue number | 2 |
| DOIs | |
| State | Published - Aug 1982 |
ASJC Scopus subject areas
- Biophysics
- Biochemistry
- Molecular Biology
- Cell Biology
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Chance, B., Moore, J., Powers, L., & Ching, Y. (1982). A redox equilibrator for the preparation of cytochrome oxidase of mixed valence states and intermediate compounds for X-ray synchrotron studies. Analytical Biochemistry, 124(2), 239-247. https://doi.org/10.1016/0003-2697(82)90034-3