Lithium borate gel films prepared from aqueous solution

J. D. Hemry, M. C. Weinberg, Donald R Uhlmann

Research output: Contribution to journalArticle

1 Citation (Scopus)

Abstract

Transparent, durable films of lithium diborate gel can easily be prepared on a variety of substrates from supersaturated aqueous solutions of lithium hydroxide monohydrate and boric acid by spin-coating. The gel to dried gel to glass to crystalline lithium tetraborate (Li2B4O7) transformation has been studied by infrared spectroscopy of thin films cast on potassium bromide windows. Examination by scanning electron microscopy disclosed that distinctly different crystal morphology was associated with a difference in the transformation rate observed between gel and dried gel films. Films of 250 nm to 30 μm in thickness have been produced.

Original languageEnglish (US)
Pages (from-to)3853-3858
Number of pages6
JournalJournal of Materials Science
Volume33
Issue number15
StatePublished - 1998

Fingerprint

Lithium
Gels
Boric acid
Spin coating
Potassium
Infrared spectroscopy
Borates
lithium borate
Crystalline materials
Glass
Thin films
Crystals
Scanning electron microscopy
Substrates

ASJC Scopus subject areas

  • Materials Science(all)

Cite this

Lithium borate gel films prepared from aqueous solution. / Hemry, J. D.; Weinberg, M. C.; Uhlmann, Donald R.

In: Journal of Materials Science, Vol. 33, No. 15, 1998, p. 3853-3858.

Research output: Contribution to journalArticle

Hemry, JD, Weinberg, MC & Uhlmann, DR 1998, 'Lithium borate gel films prepared from aqueous solution', Journal of Materials Science, vol. 33, no. 15, pp. 3853-3858.
Hemry, J. D. ; Weinberg, M. C. ; Uhlmann, Donald R. / Lithium borate gel films prepared from aqueous solution. In: Journal of Materials Science. 1998 ; Vol. 33, No. 15. pp. 3853-3858.
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