1H and 13C NMR signal assignments of a novel Baeyer-Villiger originated diterpene lactone

Henriete S. Vieira, Jacqueline A. Takahashi, A. A.Leslie Gunatilaka, Maria Amélia D. Boaventura

Research output: Contribution to journalArticle

4 Scopus citations

Abstract

A highly rearranged novel dilactone was the single product isolated from Baeyer-Villiger oxidation of a norketone prepared from grandiflorenic acid, a natural kaurane diterpene. The complete 1H and 13C NMR assignment is presented for this novel compound that showed discrete in vitro antibacterial activity.

Original languageEnglish (US)
Pages (from-to)146-150
Number of pages5
JournalMagnetic Resonance in Chemistry
Volume44
Issue number2
DOIs
StatePublished - Feb 1 2006

Keywords

  • 1D NMR
  • 2D NMR
  • Baeyer-Villiger oxidation
  • Kaurane diterpene lactones

ASJC Scopus subject areas

  • Chemistry(all)
  • Materials Science(all)

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