Synthesis and characterization of tetrathiatetraasterane

Nina V. Bojkova, Richard S. Glass

Research output: Contribution to journalArticle

8 Scopus citations

Abstract

Irradiation of 1,4-dithiin gives the cis, syn, cis-photodimer in 70-80% yield whose structure has been unequivocally established by X-ray crystallographic methods. A minor product is formed in this photodimerization which is shown to the trans, anti, trans-photodimer by X-ray structural analysis. Irradiation of the syn photodimer produces tetrathiatetraasterane in 70% yield. The structure of this product is also proven by X-ray methods.

Original languageEnglish (US)
Pages (from-to)9125-9126
Number of pages2
JournalTetrahedron Letters
Volume39
Issue number50
DOIs
StatePublished - Dec 10 1998

ASJC Scopus subject areas

  • Biochemistry
  • Drug Discovery
  • Organic Chemistry

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