Synthesis of 1,10-dimethylbicyclo[8.8.8]hexacosane and 1,10- dihydroxybicyclo[8.8.8]hexacosane

Ian W. Jones, Yasunari Monguchi, Alice Dawson, Michael D. Carducci, Eugene A. Mash

Research output: Contribution to journalArticle

4 Scopus citations

Abstract

(Chemical Equation Presented) 1,10-Dimethylbicyclo[8.8.8]hexacosane (1) and 1,10-dihydroxybicyclo[8.8.8]hexacosane (2) were prepared in 4% yield over seven steps and in 18% yield over three steps, respectively, starting from 1,10-cyclooctadecanedione. The identities and out,out conformations of these compounds were established by single-crystal X-ray analysis.

Original languageEnglish (US)
Pages (from-to)2841-2843
Number of pages3
JournalOrganic Letters
Volume7
Issue number14
DOIs
StatePublished - Jul 7 2005

ASJC Scopus subject areas

  • Biochemistry
  • Physical and Theoretical Chemistry
  • Organic Chemistry

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