Tert-Butyl 4-(3,4-dichloroanilino)piperidine-1-carboxylate

Mehr-Un-Nisa; Munawar Ali Munawar; Gabriel B. Hall; Sue A. Roberts; Victor J. Hruby

doi:10.1107/S1600536812051896

Tert-Butyl 4-(3,4-dichloroanilino)piperidine-1-carboxylate

Mehr-Un-Nisa, Munawar Ali Munawar, Gabriel B. Hall, Sue A. Roberts, Victor J. Hruby

Chemistry and Biochemistry

Research output: Contribution to journal › Article

Abstract

In the title compound, C₁₆H₂2Cl2N₂O ₂, the substituted piperidine ring adopts a chair conformation with both substituents in equatorial positions. In the crystal, N - H⋯O and C - H⋯O hydrogen bonds connect molecules into ribbons along the a-axis direction.

Original language	English (US)
Pages (from-to)	o205
Journal	Acta Crystallographica Section E: Structure Reports Online
Volume	69
Issue number	2
DOIs	https://doi.org/10.1107/S1600536812051896
State	Published - Feb 1 2013

Keywords

R factor = 0.034
T = 100 K
data-to-parameter ratio = 65.3
mean σ(C-C) = 0.001 Å
single-crystal X-ray study
wR factor = 0.079

ASJC Scopus subject areas

Chemistry(all)
Materials Science(all)
Condensed Matter Physics

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Mehr-Un-Nisa, Munawar, M. A., Hall, G. B., Roberts, S. A., & Hruby, V. J. (2013). Tert-Butyl 4-(3,4-dichloroanilino)piperidine-1-carboxylate. Acta Crystallographica Section E: Structure Reports Online, 69(2), o205. https://doi.org/10.1107/S1600536812051896

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abstract = "In the title compound, C16H22Cl2N2O 2, the substituted piperidine ring adopts a chair conformation with both substituents in equatorial positions. In the crystal, N - H⋯O and C - H⋯O hydrogen bonds connect molecules into ribbons along the a-axis direction.",

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T1 - Tert-Butyl 4-(3,4-dichloroanilino)piperidine-1-carboxylate

AU - Mehr-Un-Nisa,

AU - Munawar, Munawar Ali

AU - Hall, Gabriel B.

AU - Roberts, Sue A.

AU - Hruby, Victor J.

PY - 2013/2/1

Y1 - 2013/2/1

N2 - In the title compound, C16H22Cl2N2O 2, the substituted piperidine ring adopts a chair conformation with both substituents in equatorial positions. In the crystal, N - H⋯O and C - H⋯O hydrogen bonds connect molecules into ribbons along the a-axis direction.

AB - In the title compound, C16H22Cl2N2O 2, the substituted piperidine ring adopts a chair conformation with both substituents in equatorial positions. In the crystal, N - H⋯O and C - H⋯O hydrogen bonds connect molecules into ribbons along the a-axis direction.

KW - R factor = 0.034

KW - T = 100 K

KW - data-to-parameter ratio = 65.3

KW - mean σ(C-C) = 0.001 Å

KW - single-crystal X-ray study

KW - wR factor = 0.079

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JO - Acta Crystallographica Section E: Structure Reports Online

JF - Acta Crystallographica Section E: Structure Reports Online

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